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Journal Articles

Spark plasma sintering of SiC/graphite functionally graded materials

Watanabe, Masashi; Yokoyama, Keisuke; Imai, Yoshiyuki; Ueta, Shohei; Yan, X.

Ceramics International, 48(6), p.8706 - 8708, 2022/03

 Times Cited Count:8 Percentile:72.1(Materials Science, Ceramics)

Previous studies have used various methods for sintering of SiC, carbon, and SiC/carbon functionally graded materials (FGM). However, no experimental studies on SiC/graphite FGM manufacturing using the spark plasma sintering (SPS) method have been reported. In this study, a SiC/graphite FGM specimen has been fabricated using SPS. The interface between the adjacent layers of the sintered specimen exhibits no apparent defects such as gaps or delaminations. The SiC and graphite phases in the specimen show no substantial change before and after sintering.

Journal Articles

Residual stress measurement by neutron diffraction methode and computation of FEM

Inoue, Kazuko*; Nakamura, Hiroshi*; Horikawa, Takeshi*; Kawashima, Hisakazu*; Tsujikami, Tetsuya*; Minakawa, Nobuaki

Nihon Zairyo Gakkai Dai-50-Ki Gakujutsu Koenkai Koen Rombunshu, p.415 - 416, 2001/05

no abstracts in English

JAEA Reports

Formation and evaluation of functionally gradient material for thermal stress relaxation, 1

; Hirakawa, Yasushi; Kano, Shigeki; Yoshida, Eiichi

PNC TN9410 98-048, 56 Pages, 1998/03

PNC-TN9410-98-048.pdf:7.03MB

Planar specimens of functionally gradient material (FGM) for thermal stress relaxation in fast reactor environment were formed and evaluated. FGMs of Al$$_{2}$$O$$_{3}$$-SUS316L system and Y$$_{2}$$O$$_{3}$$-SUS316L system were deposited on SUS316L substrates by low pressure plasma spraying. The deposited coatings with 6 layers in which the ratio of ceramics/SUS316FR changes from 0 to 100% by 20% were successfully formed. Cross-sectional observation of the coatings showed no cracks and the hardness in the coating increased continuously from the substrate to the surface. From the results of X-ray diffraction, there were no changes in the structure of SUS316L and Y$$_{2}$$O$$_{3}$$ between the powder and the coating. On the contrary, in the case of Al$$_{2}$$O$$_{3}$$, $$gamma$$ - Al$$_{2}$$O$$_{3}$$ phase was detected in the coating formed from $$alpha - Al$$_${2}$$$O$$_${3}$$ powder. The specimens were exposed in liquid sodium at 823K or 923K for 3.6Ms(1000h). The coatings were damaged with many cracks in liquid sodium. It was revealed that the bonding strength between the sprayed particles were not sufficient. To improve the stability in liquid sodium, another specimens were formed with changing the chamber pressure during deposition. From the microstructural inspections of the specimens, the coating formed at higher chamber pressure showed less porosity.

Journal Articles

Preliminary characterization of interlayer for Be/Cu functionally gradient materials; Thermophysical properties of Be/Cu sintered compacts

Saito, Shigeru; *; *; Kawamura, Hiroshi

Functionally Graded Materials 1996, 0, p.215 - 220, 1996/00

no abstracts in English

JAEA Reports

Report of phase I program (1989$$sim$$1993) on nuclear material crossover research

Kano, Shigeki; Tachi, Yoshiaki; ; ; Yoshida, Eiichi; Hirakawa, Yasushi

PNC TN9410 94-113, 70 Pages, 1994/04

PNC-TN9410-94-113.pdf:3.67MB

(Purpose) This report describes the outline, research results obtained, interchange activities, etc. of the Phase I Program on the Nuclear Material Crossover Research, which has been conducted by related research institutes including PNC/OEC from 1989 through 1993 fiscal year, and shows the Phase II Program to be started from 1994 fiscal year. (Method) Crossover research programs, research results and interchange methods were decided through discussions at the crossover research comittee (chairman : Prof.M.Okamoto, TIT) in which PNC, JAERI, NRIM, NIRIM and NCLI were participated as main members. Forums, seminars, symposiums and workshops with domestic and foreign experts on materials research were set up as the opportunities for interchange. (Results) (1)As secretary institutes, PNC and JAERl planned eight times of forums, 3 times of seminars, twice of domestic symposiums, once of international symposium, five workshops with research institutes in France, Germany, Italy and the Netherland. The contacts with outside experts, collection of new information on advanced materials, receipt of test samples, achievement of collaborative research, etc. through these interchanges were much valuable for effective performance of PNC research. (2)The following results were obtained on PNC research. The prospects on creation of following advanced materials were obtained through these interchanges: (a)advanced ceramics having excellent corrosion resistance to sodium, (b)longer life neutron absorbing materials having higher resistance to cracking than B$$_{4}$$C, (c)high performance shielding materials having higher heat resistance than conventional materials. (3)Phase II Program to be started from 1994 fiscal year has been planned by main five institutes and authorized through the evaluation by two evaluation comittees organized separately by the crossover research comittee and PNC. (Conclusion) The prospects on creation of several advanced materials were obtained through ...

JAEA Reports

Fabrication and evaluation of the tubed functionally gradient material by slurry dipping

Watanabe, Ryuzo*; *

PNC TJ9601 94-003, 87 Pages, 1994/03

PNC-TJ9601-94-003.pdf:4.58MB

This report is the PNC contract research for fiscal year of 1993 titled "Formation of Ti/SUS/Mo graded layer by slurry dipping." Fuel sheath material for FBR is used under a severe enviroment. The life of conventionally used SUS316 is known to be only two years. The development of long-life core material having high temperature strength, radiation resistance and anti-corrosion property is now essential. To create a super-long-life core materials for FBR it seems promising to employ the concept of functionally gradient material, in which these different materials are configurated with grading : as base material is used SUS316 stainless steel, the inner wall is made of Ti for the radiation resistant and anti-corrosion property with graded intermediate layers towards the base metal and the outer shell is the graded Mo layer for the corrosion resistance against liquid sodium. The shape of the core tube is a long cylindrical tube and its dimensions are 8.5mm in outer diameter, about 2m in length, shell thickness is 0.5mm and the thickness of the gradient layer is about 0.1mm. However, we have not yet acquired sufficient techniques to realize such shape and dimmensions, and the investigation is planned to get basic informations on the processing of the core materials with graded structures. Slurry dipping has been employed for forming a graded layer on curved inner and outer surfaces. And it is indispensable that the graded layers have showed sufficient thermal-stress relief function, as well as good bonding capability. In this year (FY 1993), the formation of the graded inner layer of Ti/SUS316 by slurry dipping was investigated. The formation procedure is briefly mentioned here as follows. Cylindrical green compacts of SUS304 stainless steel powder was prepared by die compaction and CIP as a substrate for slurry dipping. A coarse Ti powder was suspended in ethanol and milled by tumbler ball mill to get a slurry having an appropriate viscosity for dipping. The ...

Journal Articles

Development and experiences with JT-60U plasma facing components

Ando, Toshiro

NIFS-PROC-12, p.75 - 78, 1993/03

no abstracts in English

Journal Articles

Improvement of oxidation resistance of carbon and graphite materials by compositionally gradient SiC/C layer

Shindo, Masami

Keisha Kino Zairyo, 0(19), p.14 - 17, 1992/12

no abstracts in English

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